SAXS, WAXS, SWAXS & XRD on lab instruments and at synchrotron radiation beamlines.

Nanomaterial analysis: Nanoparticle size distribution and nanostructure analysis using X-ray methods. PANalytical.

Professional Interests | Biography | Publications | Selected Research Results

 

 

 

 

Joerg Bolze

Dr. rer. nat.

 

 

 

Eskerplein 163

7603 WH Almelo

The Netherlands
 

Tel.

 +31 546 795364

 

   

                                          

 

PROFESSIONAL INTERESTS

 

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 BIOGRAPHY

Listed in 'Who's Who in Science and Engineering' (invited)

Listed in 'Living Science', IBC Cambridge (invited)

 

 

Since 10/2011   Segment Manager - Nanomaterials

PANalytical B.V., Almelo / THE NETHERLANDS

A) X-ray diffraction, scattering and spectroscopic techniques for nanomaterial analysis
B)

Development of SAXS/WAXS options on multi-purpose X-ray diffractometer platforms

(Empyrean and X'Pert Powder and X'Pert PRO MPD from PANalytical)

B) Small-angle X-ray scattering software development (EasySAXS from PANalytical)

 

 

 11/2006 - 09/2001   Application Specialist SAXS & XRD

PANalytical B.V., Almelo / THE NETHERLANDS

A) Product and application development
B) Nanostructure and nanoparticle size distribution analysis.

 

 

 10/2003 - 10/2006   Application Chemist / Product Manager

Interpolymer Sàrl, Technical Service Group, Wissembourg / FRANCE

A)

Specialty polymers and polymer dispersions in paints, coatings, water treatment, floor care, carpet care, etc. Formulation development and application tests for decorative paints, wood lacquers and floor polishes.

B)

Technical support for Asian and European customers.  Business development and marketing.

 

 

 11/2001 - 09/2003   Colloid Researcher

Universität Karlsruhe (TH), Polymer-Institute, Group of Prof. M. Ballauff,  GERMANY

A)

Structural investigations on industrial core-shell polymer latex particles.

Background: Structure-property correlation.

B)

Analysis of the formation and growth of colloidal calcium carbonate particles from supersaturated salt solutions by time-resolved synchrotron small- and wide-angle X-ray scattering.

Background: Mechanism of particle formation; biomineralization; industrial crystallization; incrustation inhibition by polymer additives.

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C)

Structural investigations on bio-functionalized latex particles.

Background: Latex agglutination tests; bioassays; latex spheres as smart carrier particles for drug targeting.

 

 

 03/2000 - 09/2001   Senior Polymer Researcher

Pohang University of Science and Technology (POSTECH),  Pohang / KOREA:

Polymer Research Institute and Pohang Accelerator Laboratory

  - Member of the Korean Polymer Society -

A)

Characterized nanoporous, low-dielectric-constant poly(organosilicate)-films as well as poly(organosilicate) / poly(caprolactone) hybrid films by X-ray reflectivity and ellipsometry.

Background: Development of advanced low-dielectric-constant materials for the semiconductor industry. Sol-gel process, spin-on glasses, organic/inorganic hybrid materials. X-ray reflectivity as a tool for the determination of the mass density and porosity in thin (sub-micrometer) films.

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B)

Tested, upgraded and used a small-angle X-ray scattering beamline dedicated to the structural analysis of polymers and colloids. Investigated the performance of various X-ray detection systems. 

Background: High-flux synchrotron X-ray radiation for new applications in colloid and polymer science.

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 11/1997 - 02/2000   Post-Doctor

 

The Institute of Physical and Chemical Research (RIKEN),  Harima / JAPAN:

Structural Biophysics Laboratory / Synchrotron X-ray source SPring-8

Collaborated with the Max-Planck Inst. for Polymer Res. (Prof. W. Knoll), Mainz

  - Member of the Japanese Biophysical Society -

A)

Characterized the structure of lipopolymer Langmuir-Blodgett films (polymer supported lipid bilayers) under controlled humidity by X-ray reflectivity and grazing incidence, in-plane X-ray diffraction.

Background: Model biomembranes; biocompatibilization of solid surfaces.

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B)

Applied synchrotron small-angle X-ray scattering and 31P NMR for studying the phase behavior of DMPC/DHPC bicelles (bilayered lipid micelles).

Background: Bicelles as a biomimetic, diamagnetic matrix for proteins that are to be studied by high resolution NMR.

C)

Supported the commissioning of a synchrotron small-angle X-ray scattering beamline: test measurements on aqueous polymer dispersions and surfactants.

Background: Very high-flux synchrotron X-ray radiation for new applications in colloid and polymer science (e.g. kinetic measurements, high-pressure research).

 

 

 08/1997 - 10/1997  Frontier Researcher

The Institute of Physical and Chemical Research (RIKEN),  Wako / JAPAN:

Laboratory of Exotic Nano-Materials, International Frontier Research Program

A)

Learned about the modification and characterization of solid surfaces on a molecular level.

Background: Biocompatibilization of surfaces.

 

 

 04/1994 - 06/1997   Scientific Employee

Universität Karlsruhe (TH), Polymer-Institute, Group of Prof. M. Ballauff,  GERMANY

A)

Investigated on the adsorption of anionic and nonionic surfactants on the surfaces of polymer latex particles using small-angle X-ray scattering in combination with the contrast variation method.

Background: Particle stabilization; competitive adsorption.

B)

Analysed the structure of PMMA latex particles swollen with various monomers by small-angle X-ray scattering in combination with the contrast variation method.

Background: Wall-repulsion effect; mechanism of emulsion polymerization.

C)

Participated in industrial projects: preparation, characterization and application of core-shell latexes.

Background: Structure-property correlation.

 

 

 1991   Polymer Research Associate (9 weeks)

Korea Institute of Science and Technology (KIST),  Seoul / KOREA

  - Scholarship sponsered by Deutscher Akademischer Austauschdienst (DAAD) -

A)

Worked on liquid crystalline polymers and polymer composites.

 

 

 

 Education:

 

 10/1987 - 04/1997   Chemistry Student

Universität Karlsruhe, Dept. of Chemistry,  GERMANY

A)

Focused on polymer science and physical chemistry with additional education in physics, mathematics and computer science.

B)

Studied the Japanese and Chinese languages for several years.

Passed the Japanese Language Proficiency Test (Level 3) of the Japan Foundation in 1995.

 

 

 04/1994 - 04/1997   Doctoral Thesis

Polymer-Institute   (Prof. M. Ballauff)
Title:  

"Structural investigations on polymer colloids: Analysis of adsorption

and swelling equilibria by small angle X-ray scattering."

 

 

 08/1993 - 02/1994   Diploma Thesis

Polymer-Institute   (Prof. M. Ballauff)

Title:  

"Contrast variation in small angle X-ray scattering: Structural investigations

on swollen polymer latexes."

 

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 PUBLICATIONS

 

18.

V. Kogan, D. Beckers, J. Bolze, C. W. Lehmann, H. G. Schweim, K.-J. Steffens

 

US Patent  20090232276

European Patent  EP2090883

 

"X-ray detection in packaging."

 

17.

J. Bolze

 

Welt der Farben, April 2006.

 

"Kationische Polymerdispersionen für durchschlagende Erfolge in der Fleckenbekämpfung."

 

16.

S. Rosenfeldt, A. Wittemann, M. Ballauff, E. Breininger, J. Bolze, N. Dingenouts

 

Physical Review E 2004, 70, 061403.

 

"Interaction of Proteins with Spherical Polyelectrolyte Brushes in Solution

as Studied by Small-Angle X-Ray Scattering."

Abstract

 

 

15.

J. Bolze, D. Pontoni, M. Ballauff, T. Narayanan, H. Cölfen

 

Journal of Colloid and Interface Science 2004, 277, 84-94.

 

"Time-Resolved SAXS Study on the Effect of a Double Hydrophilic Block-Copolymer

on the Formation of CaCO3 from a Supersaturated Salt Solution."

Abstract

 

 

14.

J. Bolze, M. Ballauff, T. Rische, D. Rudhardt, J. Meixner

 

Macromoelcular Chemistry and Physics 2004, 205, 165-172.   Feature Article.

 

"In situ Structural Characterization of Semi-Crystalline Latex Particles by Small-Angle X-Ray Scattering."

Abstract and Coverpage

 

 

13.

J. Bolze, M. Ballauff, J. Kijlstra, D. Rudhardt

 

Macromolecular Materials and Engineering 2003, 288, 495-502.   Feature Article.

 

"Application of Small-Angle X-ray Scattering as a Tool for the Structural Analysis of Industrial Polymer Dispersions."

Abstract and Coverpage

 

12.

D. Pontoni, J. Bolze, N. Dingenouts, T. Narayanan, M. Ballauff

 

Journal of Physical Chemistry B 2003, 107, 5123-5125.

 

"Crystallization of Calcium Carbonate Observed In-situ by Combined Small- and Wide-Angle X-Ray Scattering."

Abstract

 

11.

J. Bolze, B. Peng, N. Dingenouts, P. Panine, T. Narayanan, M. Ballauff

 

Langmuir 2002, 18, 8364-8369.

 

"Formation and Growth of Amorphous Colloidal Calcium Carbonate Precursor Particles as Detected by Time-Resolved SAXS."

Abstract

 

10.

J. Bolze, M. Takahasi, J. Mizuki, T. Baumgart, W. Knoll

 

Journal of the American Chemical Society 2002, 124, 9412-9421.

 

"X-Ray Reflectivity and Diffraction Studies on Lipid and Lipopolymer Langmuir-Blodgett Films under Controlled Humidity." 

Abstract

 

 9.

J. Bolze, J. Kim, J.-Y. Huang, S. Rah, H. S. Youn, B. Lee, T. J. Shin, M. Ree

 

Macromolecular Research 2002, 10, 2-12.   Feature Article.

 

"Current Status of the Small-Angle X-Ray Scattering Station BL4C1 at the Pohang Accelerator Laboratory."

Full Text

 

 8.

J. Bolze, M. Ree, H. S. Youn, S.-H. Chu, K. Char

 

Langmuir 2001, 17, 6683-6691.

 

"Synchrotron X-Ray Reflectivity Study on the Structure of Templated Polyorganosilicate Thin Films  and their Derived Nanoporous Analogues."

Abstract

 

 7.

J. Bolze, T. Fujisawa, T. Nagao, K. Norisada, H. Saito, A. Naito

 

Chemical Physics Letters 2000, 329, 215-220.

 

"Small Angle X-ray Scattering and 31P NMR Studies on the Phase Behavior of Phospholipid Bilayered Mixed Micelles." 

Abstract

 

 6.

N. Dingenouts, J. Bolze, D. Pötschke, M. Ballauff

 

Advances in Polymer Science 1999, 144, 1-47.

 

"Analysis of Polymer Latexes by Small-Angle X-Ray Scattering."

Abstract

 

 5.

J. Bolze, K.D. Hörner, M. Ballauff

 

Langmuir 1997, 13, 2960-2964.

 

"Small Angle X-Ray Scattering Analysis of the Radial Structure of Latex Particles Swollen by a Nonpolar Monomer."

Abstract

 

 4.

M. Ballauff, J. Bolze, N. Dingenouts, P. Hickl, D. Pötschke

 

Macromolecular Chemistry and Physics 1996, 197, 3043-3066.

 

"Small-Angle X-Ray Scattering on Latexes."

Abstract

 

 3.

J. Bolze, K.D. Hörner, M. Ballauff

 

Colloid & Polymer Science 1996, 274, 1099-1108.

 

"Competitive Adsorption of an Anionic and a Nonionic Surfactant on Polystyrene Latex Particles as monitored by Small-Angle X-Ray Scattering."

Abstract

 

 2.

J. Bolze, K.D. Hörner, M. Ballauff

 

Langmuir 1996, 12, 2906-2912.

 

"Adsorption of the Nonionic Surfactant Triton X-405 on Polystyrene Latex Particles as monitored by Small-Angle X-Ray Scattering." 

Abstract

 

 1.

J. Bolze, M. Ballauff

 

Macromolecules 1995, 28, 7429-7433.

 

"Study of Spatial Inhomogeneities in Swollen Latex Particles by Small-Angle X-Ray Scattering: The Wall-Repulsion Effect Revisited."

Abstract                                                                                                                                                                                       

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SELECTED RESEARCH RESULTS

 

1.

Analysis of the formation and growth of colloidal calcium carbonate particles from supersaturated salt solutions by time-resolved synchrotron small-angle X-ray scattering.

 

2.

X-Ray Reflectivity and Diffraction Studies on Lipid and Lipopolymer Langmuir-Blodgett Films under Controlled Humidity.

 

3.

Synchrotron X-Ray Reflectivity Study on the Structure of Templated Polyorganosilicate Thin Films and their Derived Nanoporous Analogues.

 

4.

First Results of the commissioning of the synchrotron small-angle X-ray scattering beamline BL4C1 at the Pohang Accelerator Laboratory in Korea.

 

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Research Interests | Biography | Publications | Selected Research Results

 

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                             This site was last updated on 11.05.2012 by J. Bolze,   Almelo/The Netherlands,   joergbolze@web.de